Ethylenediamine → HCID 12635590, 화합물

반응식

[CH2:1]([NH2:4])[CH2:2][NH2:3].[Br:5][C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([Br:12])[C:7]=1[N:13]=[C:14]=[S:15]>>[NH2:3][CH2:2][CH2:1][NH:4][C:14]([NH:13][C:7]1[C:8]([Br:12])=[CH:9][CH:10]=[CH:11][C:6]=1[Br:5])=[S:15]

참가 물질

반응물 2

HCID 3301Ethylenediamine

HCID 126355872,6-Dibromophenyl isothiocyanate

생성물 1

HCID 12635590HCID 12635590, 화합물

실험 절차

In a similar manner to that described in Example 1, ethylenediamine was reacted with 2,6-dibromophenylisothiocyanate to yield 1-(2-aminoethyl)-3-(2,6-dibromophenyl)thiourea, melting point 155°-157°.

출처 및 근거

ORD 기록: ord-e539067c86c24d72b1ca90d97d77ae3d
출처 데이터셋: uspto-grants-1979_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04150138

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