Isobutyryl chloride → HCID 12556919, 화합물

HRID 26488노트

반응식

HRID 26488 반응식
[CH2:1]([NH:5][C:6]1[O:7][CH:8]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[N:10]=1)[CH2:2][CH2:3][CH3:4].[C:17](Cl)(=[O:21])[CH:18]([CH3:20])[CH3:19]>>[CH2:1]([N:5]([C:6]1[O:7][CH:8]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[N:10]=1)[C:17](=[O:21])[CH:18]([CH3:20])[CH3:19])[CH2:2][CH2:3][CH3:4]

참가 물질

3

반응물 2

HCID 62325Isobutyryl chlorideHCID 122952382-(N-Butylamino)-4-phenyloxazole

생성물 1

HCID 12556919HCID 12556919, 화합물

실험 절차

2-(N-butylamino)-4-phenyloxazole was acylated with isobutyryl chloride as described in Example 9. An almost colourless oil was obtained on distillation. WT.= 4.9 g., b.p. 140° C. (air-bath temperature)/1 mm., 80%.

후처리

  1. customAn almost colourless oil was obtained on distillation

출처 및 근거

ORD 기록
ord-f68a0d3dcc1d44c080a26dc4ec867ca8
출처 데이터셋
uspto-grants-1979_04
특허 번호
US04150143

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