Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 9-(3,4,5-Triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)nonanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Disodium acetylide | HCID 560317 | — |
| 반응물 | 1,4,5-Triphenyl-1,3-dihydro-2H-imidazol-2-one | HCID 628544 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | 9-(3,4,5-Triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)nonanoic acid | HCID 22916411 | — |
반응 단계
1,4,5-Triphenylimidazol-2-one was treated with ethyl 9-bromononanoate and potassium carbonate in butanone, followed by sodium hydroxide in ethanol and water, to give after work-up the title compound, m.p. 123°-124° C., Found:C, 76.9;H, 6.9;N, 5.7%;C30H32N2O3 requires: C, 76.9; H, 6.9; N, 6.0%
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05648373 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-875414e9de0d4c98b502bba67e1cb404 |
| 출처 메모 | uspto-grants-1997_07 |