Methyl iodide → HCID 20515175, 화합물

HRID 26549

반응식

HRID 26549 반응식
[NH2:1][C:2]1[CH:3]=[C:4]([C:14](=[O:20])[C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH:5]=[CH:6][C:7]=1[CH:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1.[CH3:21]I>N1C=CC=CC=1>[CH3:21][NH:1][C:2]1[CH:3]=[C:4]([C:14](=[O:20])[C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH:5]=[CH:6][C:7]=1[CH:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 20515218Ethyl 3-amino-4-cyclohexylphenylglyoxylate

생성물 1

HCID 20515175HCID 20515175, 화합물

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

To a solution of 0.01 moles of ethyl 3-amino-4-cyclohexylphenylglyoxylate in 100 ml. of pyridine is added 0.1 moles of methyl iodide. The reaction mixture is stirred overnight at room temperature, filtered and concentrated. The residue is distilled to obtain ethyl 3-methylamino-4-cyclohexylphenylglyoxylate.

후처리

  1. filtrationfiltered
  2. concentrationconcentrated
  3. distillationThe residue is distilled

출처 및 근거

ORD 기록
ord-a2e369448a4f40eea2bd19b445797bbb
출처 데이터셋
uspto-grants-1979_04
특허 번호
US04150148

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