5,5'-Bi-2-benzofuran-1,1',3,3'-tetrone → Bpda tfmb

HRID 265914

반응식

HRID 265914 반응식
[CH:1]1[C:6]([C:7]2[CH:12]=[CH:11][C:10]3[C:13]([O:15][C:16](=[O:17])[C:9]=3[CH:8]=2)=[O:14])=[CH:5][C:4]2[C:18]([O:20][C:21](=[O:22])[C:3]=2[CH:2]=1)=[O:19].[CH:23]1[C:28]([NH2:29])=[CH:27][C:26]([C:30]([F:33])([F:32])[F:31])=[C:25]([C:34]2[CH:39]=[CH:38][C:37]([NH2:40])=[CH:36][C:35]=2[C:41]([F:44])([F:43])[F:42])[CH:24]=1>CN1C(=O)CCC1>[CH:1]1[C:6]([C:7]2[CH:12]=[CH:11][C:10]3[C:13]([O:15][C:16](=[O:17])[C:9]=3[CH:8]=2)=[O:14])=[CH:5][C:4]2[C:18]([O:20][C:21](=[O:22])[C:3]=2[CH:2]=1)=[O:19].[CH:38]1[C:37]([NH2:40])=[CH:36][C:35]([C:41]([F:44])([F:42])[F:43])=[C:34]([C:25]2[CH:24]=[CH:23][C:28]([NH2:29])=[CH:27][C:26]=2[C:30]([F:31])([F:32])[F:33])[CH:39]=1

참가 물질

4

반응물 2

HCID 754945,5'-Bi-2-benzofuran-1,1',3,3'-tetroneHCID 629349(1,1'-Biphenyl)-4,4'-diamine, 2,2'-bis(trifluoromethyl)-

생성물 1

HCID 131720099Bpda tfmb

시약·촉매·용매 1

HCID 13387N-methyl-2-pyrrolidone용매

실험 절차

A solution of polyamic acid was prepared at room temperature by combining 1.215 grams of 6FDA, 2.395 grams of BPDA, 3.476 grams of TFMB and 28.7 grams of NMP with good mixing. The amic acid solution was diluted to 10% solids, then cast on a silicon wafer by spin coating, and imidized by a heat treatment up to a maximum temperature of 300° C. to produce a coating having a thickness of 1.9 microns. The refractive index was determined in the same manner as in Example 1 and is reported in Table I.

후처리

  1. customA solution of polyamic acid was prepared at room temperature
  2. customimidized by a heat treatment up to a maximum temperature of 300° C.
  3. customto produce a coating

출처 및 근거

ORD 기록
ord-2f2f69d7117b4bf6a7b79b0bfca94053
출처 데이터셋
uspto-grants-1997_07
특허 번호
US05649045

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