Triethyl phosphonoacetate → HCID 178473138, 화합물
반응식
[CH2:1]([O:3][C:4](=[O:14])[CH2:5][P:6](OCC)([O:8][CH2:9][CH3:10])=[O:7])[CH3:2].P(Cl)(Cl)(Cl)(Cl)[Cl:16].C(OC(=O)CP(OCC)(Cl)=O)C>C1C=CC=CC=1>[CH2:1]([O:3][C:4](=[O:14])[CH2:5][PH:6]([O:8][CH2:9][CH2:10][Cl:16])=[O:7])[CH3:2]참가 물질
5
실험 절차
Ethyl(diethoxyphosphinyl)acetate (11.2 gm., 0.05 mol.) and phosphorus pentachloride (10.5 gm., 0.05 mol.) are dissolved in 200 ml. of benzene and refluxed overnight. The solvent is removed in vacuo, leaving yellow, oily, ethyl(ethoxychlorophosphinyl)acetate as residue (11.5 gm.).
후처리
- customThe solvent is removed in vacuo
- customleaving yellow
출처 및 근거
- ORD 기록
- ord-f5f7c881caa9453e8959c0b4ff68e9d8
- 출처 데이터셋
- uspto-grants-1979_04
- 특허 번호
- US04151172
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