HCID 53844855, 화합물 → 3-acetoxy-3-(N-acetylisopropylaminomethyl)-7-amino-3,4-dihydro-2H-1,5-benzodioxepin

HRID 267774노트

반응식

HRID 267774 반응식
[C:1]([O:4][C:5]1([CH2:19][N:20]([CH:24]([CH3:26])[CH3:25])[C:21](=[O:23])[CH3:22])[CH2:11][O:10][C:9]2[CH:12]=[CH:13][C:14]([N+:16]([O-])=O)=[CH:15][C:8]=2[O:7][CH2:6]1)(=[O:3])[CH3:2].[H][H]>C(OCC)(=O)C.[Pt]>[C:1]([O:4][C:5]1([CH2:19][N:20]([CH:24]([CH3:26])[CH3:25])[C:21](=[O:23])[CH3:22])[CH2:11][O:10][C:9]2[CH:12]=[CH:13][C:14]([NH2:16])=[CH:15][C:8]=2[O:7][CH2:6]1)(=[O:3])[CH3:2]

참가 물질

5

반응물 2

HCID 53844855HCID 53844855, 화합물HCID 178418361HCID 178418361, 화합물

생성물 1

HCID 540731773-acetoxy-3-(N-acetylisopropylaminomethyl)-7-amino-3,4-dihydro-2H-1,5-benzodioxepin

시약·촉매·용매 2

HCID 23939Platinum촉매HCID 8857Ethyl Acetate용매

실험 절차

The 3-acetoxy-3-(N-acetylisopropylaminomethyl)-7-nitro-3,4-dihydro-2H-1,5-benzodioxepin when dissolved in ethyl acetate is reduced at low pressure over platinum with hydrogen to give 3-acetoxy-3-(N-acetylisopropylaminomethyl)-7-amino-3,4-dihydro-2H-1,5-benzodioxepin.

출처 및 근거

ORD 기록
ord-1be76147e9bd4e39a51a1b1a9e1a1b39
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03944560

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