Benzylamine → N-benzyladamantane-1-carboxamide

HRID 267876

반응식

HRID 267876 반응식
[C:1]12([C:11](Cl)=[O:12])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[CH2:14]([NH2:21])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>C(OCC)C>[CH2:14]([NH:21][C:11]([C:1]12[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2)=[O:12])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

참가 물질

4

반응물 2

HCID 7504BenzylamineHCID 989151-Adamantanecarbonyl chloride

생성물 1

HCID 3826889N-benzyladamantane-1-carboxamide

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

Dissolve 2.0 g. of (10 mmoles) of 1-adamantane carboxylic acid chloride in 20 ml. of ethyl ether and add to 3.0 ml. (28.0 mmoles) of benzylamine and repeat the process of Example 11 to obtain the product of this example, m.p. 170°-172°C.

후처리

  1. dissolutionDissolve 2.0 g
  2. customto obtain the product of this example, m.p. 170°-172°C.

출처 및 근거

ORD 기록
ord-370d15f0b8ad4bbdb3f3a0be1d3afd6a
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03944675

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