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Hydroxyamine hydrochloride → HCID 85436872, 화합물

HRID 268097
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인쇄 미리보기

반응식

HRID 268097 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:13][C:12]([CH:14]=O)=[CH:11][CH:10]=2)=[CH:5][CH:4]=1.Cl.[NH2:17][OH:18]>O>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:13][C:12]([CH:14]=[N:17][OH:18])=[CH:11][CH:10]=2)=[CH:5][CH:4]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 443297Hydroxyamine hydrochlorideHCID 27596555-(4-Methoxyphenyl)-2-furaldehyde

생성물 1

HCID 85436872HCID 85436872, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A 250 ml Erlenmeyer flask was charged with 5-(4-methoxyphenyl)-2-furaldehyde (40 g, 0.20 mole) and absolute alcohol (125 ml). A solution of hydroxylamine hydrochloride (14 g, 0.20 mole) in water (25 ml) was added to this suspension. This mixture was stirred for 1 hour, cooled, filtered and washed with isopropanol, yielding 28 g (65.2%).

후처리

  1. temperaturecooled
  2. filtrationfiltered
  3. washwashed with isopropanol
  4. customyielding 28 g (65.2%)

출처 및 근거

ORD 기록
ord-18d19c5b3d264278a56a40064d5153a5
출처 데이터셋
uspto-grants-1976_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US03946049

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