Acetic Anhydride → HCID 12227147, 화합물

HRID 268098노트

반응식

HRID 268098 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:13][C:12]([CH:14]=[N:15]O)=[CH:11][CH:10]=2)=[CH:5][CH:4]=1.C(OC(=O)C)(=O)C>CCOCC>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:13][C:12]([C:14]#[N:15])=[CH:11][CH:10]=2)=[CH:5][CH:4]=1

참가 물질

4

반응물 2

HCID 7918Acetic AnhydrideHCID 85436872HCID 85436872, 화합물

생성물 1

HCID 12227147HCID 12227147, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

A 500 ml three-necked flask equipped with stirrer, thermometer and reflux condenser was charged with 5-(p-methoxyphenyl)-2-furaldehyde oxime (28 g, 0.129 mole) and acetic anhydride (317 ml). This mixture was refluxed (138°) for 3 hours. After cooling to room temperature overnight, the green solution was poured into ice water (ca. 2l. ) with stirring. When the ice melted, the solid was collected by filtration, washed with water, and dried to give 26 g.

후처리

  1. customA 500 ml three-necked flask equipped with stirrer
  2. temperaturethermometer and reflux condenser
  3. temperatureThis mixture was refluxed (138°) for 3 hours
  4. filtrationthe solid was collected by filtration
  5. washwashed with water
  6. customdried
  7. customto give 26 g

출처 및 근거

ORD 기록
ord-5326d26079af4b7ca96f8d30b084d4bc
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03946049

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