반응식
ON1C(=O)CCC1=O.[OH:9][C:10]([CH2:12][CH2:13][CH2:14][CH2:15][C@H:16]1[C@@H:24]2[C@@H:19]([NH:20][C:21]([NH:23]2)=[O:22])[CH2:18][S:17]1)=[O:11].[NH2:25][CH2:26][CH2:27][C:28]1[CH:33]=[CH:32][C:31]([OH:34])=[CH:30][CH:29]=1.C(=O)(O)[O-].C([NH+](CC)CC)C>CN(C)C=O>[OH:11][C:10]([CH2:12][CH2:13][CH2:14][CH2:15][C@H:16]1[C@@H:24]2[C@@H:19]([NH:20][C:21]([NH:23]2)=[O:22])[CH2:18][S:17]1)=[O:9].[NH2:25][CH2:26][CH2:27][C:28]1[CH:33]=[CH:32][C:31]([OH:34])=[CH:30][CH:29]=1참가 물질
5
반응 조건
- 온도
- 50 °C
실험 절차
a solution of biotin-N-hydroxysuccinimide, 170 mg (0.5 mMoles), and tyramine (recrystallized from water), 68.5 mg (0.5 mMoles), in 25 ml dimethylformamide was treated with 10 ml of 1M triethylammonium bicarbonate, pH 7.5, and then heated at 50° C. for 3 hours.
출처 및 근거
- ORD 기록
- ord-989c68d91dfc4d74a9b62cfdff0165f9
- 출처 데이터셋
- uspto-grants-1998_03
- 특허 번호
- US05731158
연결된 노트
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