Phenyl formate → HCID 21552229, 화합물

HRID 268462

반응식

[CH3:1][C:2]([NH2:15])([CH2:13][CH3:14])[CH2:3][C:4]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[NH:6][CH:5]=1.[CH:16](OC1C=CC=CC=1)=[O:17]>>[CH3:1][C:2]([NH:15][CH:16]=[O:17])([CH2:13][CH3:14])[CH2:3][C:4]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[NH:6][CH:5]=1

참가 물질

반응물 2

HCID 74626Phenyl formate

HCID 21552235HCID 21552235, 화합물

생성물 1

HCID 21552229HCID 21552229, 화합물

실험 절차

The 3-(2'-methyl-2'-aminobutyl)-indole obtained as reduction product in accordance with Example 1 or 3 was reacted with phenyl formate to yield 3-(2'-methyl-2'-formylaminobutyl)-indole; melting point 121.5°-124.5°C. (from ether). Reduction thereof with LiAlH4 yielded 3-(2'-methyl-2'-methylaminobutyl)-indole having a melting point of 100°-103°C. (from cyclohexane).

출처 및 근거

ORD 기록: ord-8f956a4918304bc2a1e7c1de3a525c8b
출처 데이터셋: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03947584

연결된 노트

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