Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(3-Piperidin-1-ylpropoxy)benzoic acid hydrochloride → 4-(3-Piperidin-1-ylpropoxy)benzoyl chloride hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(3-Piperidin-1-ylpropoxy)benzoic acid hydrochloride | HCID 68963614 | — |
| 용매 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | 4-(3-Piperidin-1-ylpropoxy)benzoyl chloride hydrochloride | HCID 21852062 | 196.6% |
반응 단계
4-(3-Piperidin-1-ylpropoxy)benzoic acid hydrochloride (D2) (0.23 g) in thionyl chloride (5 ml) was heated under reflux for 1 h. The reaction mixture was then evaporated to a minimum and co-evaporated from DCM (3×10 ml) to give the title compound (D3) as a white powder (0.24 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07446103B2 |
| 출처 데이터셋 | uspto-grants-2008_11 |
| ORD ID | ord-67c8ebd31205405786cdabfc6fd90b85 |
| 출처 메모 | uspto-grants-2008_11 |