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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 268707생성일: 2026년 10월 25일

4-(3-Piperidin-1-ylpropoxy)benzoic acid hydrochloride → 4-(3-Piperidin-1-ylpropoxy)benzoyl chloride hydrochloride

https://huagongshe.com/reaction/268707

반응식

참여 물질

역할이름HCID투입량
반응물4-(3-Piperidin-1-ylpropoxy)benzoic acid hydrochlorideHCID 68963614—
용매Thionyl ChlorideHCID 24386—
생성물4-(3-Piperidin-1-ylpropoxy)benzoyl chloride hydrochlorideHCID 21852062196.6%

반응 단계

4-(3-Piperidin-1-ylpropoxy)benzoic acid hydrochloride (D2) (0.23 g) in thionyl chloride (5 ml) was heated under reflux for 1 h. The reaction mixture was then evaporated to a minimum and co-evaporated from DCM (3×10 ml) to give the title compound (D3) as a white powder (0.24 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07446103B2
출처 데이터셋uspto-grants-2008_11
ORD IDord-67c8ebd31205405786cdabfc6fd90b85
출처 메모uspto-grants-2008_11