반응식
[CH:1]([NH:5][C:6]([CH:8]=[CH:9][C:10]([OH:12])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2].Cl.[CH3:14]O>>[CH:1]([NH:5][C:6]([CH:8]=[CH:9][C:10]([O:12][CH3:14])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2]참가 물질
4
실험 절차
To 3-(sec butylcarbamoyl)acrylic acid (20 g, 117 mmol) at room temperature was added 150 mL 1.2M HCl in methanol. The resulting mixture was stirred for two hours. Solvents were removed in vacuo to give the desired ester, which was used without further purification.
후처리
- customSolvents were removed in vacuo
출처 및 근거
- ORD 기록
- ord-4c7dd66728e1478c8e5011a149f328cd
- 출처 데이터셋
- uspto-grants-2008_11
- 특허 번호
- US07449242B2
연결된 노트
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