1,1-Bis(methylthio)-2-nitroethylene → 1-Nitro-2-methylthio-2-[3-(2-oxazolylthio)propylamino]ethylene

HRID 27099

반응식

HRID 27099 반응식
[NH2:1][CH2:2][CH2:3][CH2:4][S:5][C:6]1[O:7][CH:8]=[CH:9][N:10]=1.[N+:11]([CH:14]=[C:15](SC)[S:16][CH3:17])([O-:13])=[O:12]>>[N+:11]([CH:14]=[C:15]([S:16][CH3:17])[NH:1][CH2:2][CH2:3][CH2:4][S:5][C:6]1[O:7][CH:8]=[CH:9][N:10]=1)([O-:13])=[O:12]

참가 물질

3

실험 절차

By the procedure of Example 8(i), 2-(3-aminopropylthio)oxazole (2.1 g) is reacted with 1-nitro-2,2-bis-methylthioethylene (2.0 g) to give 1-nitro-2-methylthio-2-[3-(2-oxazolylthio)propylamino]ethylene (2.1 g) which, on reaction with methylamine by the procedure of Example 8(ii) gives the title product (1.8 g).

출처 및 근거

ORD 기록
ord-db6bb7fbc6ad4f9b830b4d94e9cb2908
출처 데이터셋
uspto-grants-1980_09
특허 번호
US04220652

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