N-Ethyl cyclohexylamine → 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone

HRID 27378

반응식

HRID 27378 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:15]=[CH:16][C:17]=1Cl)[C:7]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)=[O:8])([O-:3])=[O:2].[CH2:19]([NH:21][CH:22]1[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]1)[CH3:20]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:15]=[CH:16][C:17]=1[N:21]([CH2:19][CH3:20])[CH:22]1[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]1)[C:7]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)=[O:8])([O-:3])=[O:2]

참가 물질

3

반응물 2

HCID 21609N-Ethyl cyclohexylamineHCID 417434-Chloro-3-nitrobenzophenone

생성물 1

HCID 233427783-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone

실험 절차

13 g. of 3-nitro-4-chloro-benzophenone are reacted with 15 ml. of N-ethyl-N-cyclohexylamine as described in Example 2. The crude product is recrystallized from n-hexane to yield 15.3 g of pure, crystalline 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone; m.p. 91.5°-92° C.

후처리

  1. customThe crude product is recrystallized from n-hexane

출처 및 근거

ORD 기록
ord-84ea0d37cd7e4ceea09e7d996fe0f21e
출처 데이터셋
uspto-grants-1980_09
특허 번호
US04221739

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