Sodium Hydroxide → HCID 14969707, 화합물

HRID 275338노트

반응식

HRID 275338 반응식
[NH2:1][C:2]1[N:7]=[C:6](SC)[N:5]([CH2:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:4](=[O:17])[CH:3]=1.[OH-:18].[Na+]>>[NH2:1][C:2]1[NH:7][C:6](=[O:18])[N:5]([CH2:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:4](=[O:17])[CH:3]=1

참가 물질

3

반응물 2

HCID 14798Sodium HydroxideHCID 200878306-Amino-3-benzyl-2-(methylsulfanyl)pyrimidin-4(3H)-one

생성물 1

HCID 14969707HCID 14969707, 화합물

실험 절차

Reflux 6-amino-3-(phenylmethyl)-2-methylthiopyrimidin-4(3H)-one (2.5 g=10 mmol) in 40 ml 10% aqueous NaOH for four hours. Cool, acidify the solution and collect the precipitate. Water wash and dry to give the title compound, a white solid, EI MS: M+=217.

후처리

  1. temperatureCool
  2. customcollect the precipitate
  3. washWater wash
  4. customdry

출처 및 근거

ORD 기록
ord-c7f84f230282458da550577707bb6e2e
출처 데이터셋
uspto-grants-1995_02
특허 번호
US05393755

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