Hydrogen Bromide → HCID 18316762, 화합물

반응식

[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([CH2:6][CH2:7]O)=[CH:4][CH:3]=1.[BrH:11]>>[BrH:11].[Br:11][CH2:7][CH2:6][C:5]1[CH:9]=[CH:10][C:2]([NH2:1])=[CH:3][CH:4]=1

참가 물질

반응물 2

HCID 260Hydrogen Bromide

HCID 669044-Aminophenethyl alcohol

생성물 1

HCID 18316762HCID 18316762, 화합물

실험 절차

To 4-aminophenethyl alcohol (25 g) was added 48% hydrobromic acid (250 ml), and the mixture was heated under reflux for 4 hours with stirring. After cooling, collection of the resulting precipitates by filtration gave 4-(2-bromoethyl)aniline hydrobromide (30.3 g).

후처리

temperaturethe mixture was heated
temperatureunder reflux for 4 hours
temperatureAfter cooling
customcollection of the resulting
customprecipitates by filtration

출처 및 근거

ORD 기록: ord-027a6f8cf9374d9aa80d0ab52f08ffe0
출처 데이터셋: uspto-grants-2002_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06353025B1

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