Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 3-chloro-4-hydroxyphenylacetate → 3-Chloro-4-(3'-chloro-4'-isobutoxybenzyloxy) phenylacetic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 3-chloro-4-hydroxyphenylacetate | HCID 92625 | — |
| 반응물 | 3-Chloro-4-isobutyoxybenzyl chloride | HCID 12347939 | — |
| 용매 | Methanol--water (1/1) | HCID 22242641 | — |
| 생성물 | 3-Chloro-4-(3'-chloro-4'-isobutoxybenzyloxy) phenylacetic acid | HCID 53758658 | — |
반응 단계
The procedure of Example (1) (e) was repeated wherein 3-chloro-4-isobutyoxybenzyl chloride was reacted with methyl 3-chloro-4-hydroxyphenylacetate to yield 3-chloro-4-(3'-chloro-4'-isobutoxybenzyloxy) phenylacetic acid (52.4yield), m.p. 127.5°-129° C. (methanol-water).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04221919 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-ed19a95cc9c14b48830e71430588f306 |
| 출처 메모 | uspto-grants-1980_09 |