참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | (4-Phenoxyphenyl)methanol | HCID 826195 | — |
| 생성물 | 1-(Chloromethyl)-4-phenoxybenzene | HCID 520994 | 97.2% |
반응 단계
Thionyl chloride (13.34 g) was added to 4.06 g of 4-phenoxybenzyl alcohol, and the mixture was stirred at 80° C. for 3.5 hours. After the completion of the concentration, the reaction mixture was extracted with ethyl acetate and with water. The organic layer was concentrated to give 4.31 g of 4-phenoxybenzyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06352985B1 |
|---|
| 출처 데이터셋 | uspto-grants-2002_03 |
|---|
| ORD ID | ord-e48630886bf3471b8d19ba088efbd56b |
|---|
| 출처 메모 | uspto-grants-2002_03 |
|---|
