Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Toluenesulfonyl chloride → 5-Phenylpentyl p-toluenesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 5-Phenyl-1-pentanol | HCID 61523 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 5-Phenylpentyl p-toluenesulfonate | HCID 15249503 | 102.8% |
반응 단계
To a solution of 5-phenyl-1-pentanol (3.28 g, 20 mmoles) and triethylamine (6.13 ml, 44 mmoles) in CH2Cl2 (35 ml) under N2, p-toluen-sulphonyl chloride (4.19 g, 22 mmoles) was added and then put under stirring up to room temperature for 1 night. The mixture was washed with water, NaHCO3 and 5% HCl, anhydrified and brought to dryness to give 6.55 g of the title compound (yield: 100%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06358973B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-02b648232c2e4188946f7fce31d6ec3d |
| 출처 메모 | uspto-grants-2002_03 |