Acrylamide → Prop-2-enimidic acid--2-(dimethylamino)ethyl 2-methylprop-2-enoate (1/1)

반응식

[CH3:1][C:2]([C:4]([O:6][CH2:7][CH2:8][N:9]([CH3:11])[CH3:10])=[O:5])=[CH2:3].[C:12]([NH2:16])(=[O:15])[CH:13]=[CH2:14]>>[C:12]([NH2:16])(=[O:15])[CH:13]=[CH2:14].[CH3:3][C:2]([C:4]([O:6][CH2:7][CH2:8][N:9]([CH3:11])[CH3:10])=[O:5])=[CH2:1]

참가 물질

반응물 2

HCID 6579Acrylamide

HCID 17869(Dimethylamino)ethyl methacrylate2회

생성물 1

HCID 160008Prop-2-enimidic acid--2-(dimethylamino)ethyl 2-methylprop-2-enoate (1/1)

반응 조건

온도: 85 °C

실험 절차

This example demonstrates the effect of reaction temperature on the quat content. Example 9C was repeated except that the temperature was raised to 85° C. before the initiator was added. After 6 hours G.L.C. analysis showed no DMAEMA and no acrylamide present. This indicates that none of the DMAEMA had been quaternized.

후처리

customthe effect of reaction temperature on the quat content
additionwas added

출처 및 근거

ORD 기록: ord-b4024651ddb646fda3b64ce73c2962c6
출처 데이터셋: uspto-grants-1980_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04224150

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