Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Bromo-1-indanone → 1H-inden-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Bromo-1-indanone | HCID 11745912 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 1H-inden-1-one | HCID 11815384 | — |
반응 단계
3-Bromoindan-1-one (1.5) was dissolved in diethyl ether (10 ml). The temperature was kept at +2-+4 while TEA (2.7 ml) was added. The resulting mixture was further stirred at +2-+4 for 2 hours. The precipitated salt was filtered off and the filtrate evaporated. The crude inden-1-one was used for further reaction without purification. Yield was 0.9 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06362211B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-099caa22924f4e3cb6b0fef9973b9406 |
| 출처 메모 | uspto-grants-2002_03 |