Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Phenylhydroxylamine → 1-(4-chlorophenyl)-N-phenylmethanimine oxide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Phenylhydroxylamine | HCID 7518 | — |
| 반응물 | N-(p-Chlorobenzylidene)-2-methyl-4-chloroaniline | HCID 13017552 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 1-(4-chlorophenyl)-N-phenylmethanimine oxide | HCID 254504 | — |
반응 단계
N-phenylhydroxylamine (0.052 mole) was dissolved in ether (20 cc). This solution was treated with N-(p-chlorobenzylidene)-2-methyl-4-chloroaniline (13.8 g.) dissolved in ether (50 cc). After 15 min., white crystals had begun to form. Filtration and washing with ether gave α-p-chlorophenyl-N-phenylnitrone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04224340 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-0e12529043b64c969cf8dc80bad688c5 |
| 출처 메모 | uspto-grants-1980_09 |