Sodium Fluoride → Phenyl Fluoroformate
반응식
[C:1]1([O:7][C:8](Cl)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[F-:11].[Na+].C1OCCOCCOCCOCCOC1>C(#N)C>[C:1]1([O:7][C:8]([F:11])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1참가 물질
5
반응 조건
- 온도
- 40 °C
실험 절차
To a solution of phenylchloroformate in acetonitrile is charged sodium fluoride. To this mixture is charged the 15-crown-5(“15C5”) at ambient temperature. The reaction mixture is then heated to 40° C. for approximately 16 hrs. Reaction completion is monitored by gas chromatography (“G.C.”).
후처리
- customReaction completion
출처 및 근거
- ORD 기록
- ord-550de413773c49dd9b5b621e9b040826
- 출처 데이터셋
- uspto-grants-2002_03
- 특허 번호
- US06362363B1
반응 노트
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