Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
P-Toluic Acid → (4-Methoxyphenyl)(4-methylphenyl)methanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | P-Toluic Acid | HCID 7470 | — |
| 반응물 | Anisole | HCID 7519 | — |
| 반응물 | Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1) | HCID 45075687 | — |
| 용매 | Chlorobenzene | HCID 7964 | — |
| 생성물 | (4-Methoxyphenyl)(4-methylphenyl)methanone | HCID 32113 | 7% |
반응 단계
In like manner to Example 8, anisole and para-toluic acid were reacted together (4 hour reflux) in chlorobenzene in the presence of ytterbium (III) trifluoromethanesulfonate hydrate, to give crude 4-methoxy-4′-methylbenzophenone (0.15 g, 7% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06362375B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-e9e79e661c064ff391d37c8d1f599ad8 |
| 출처 메모 | uspto-grants-2002_03 |