huagongshe.com
HRID279700

反应详情

EQUATION

反应方程式

HRID 279700 的结构方程式

REACTANTS

反应物

3
结构：Cc1ccc(C(=O)O)cc1
HCID7470

4-Methylbenzoic acid

C8H8O2

结构：COc1ccccc1
HCID7519

Anisole

C7H8O

结构：O.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]
HCID45075687

Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)

C3H2F9O10S3Yb

PRODUCTS

生成物

1
结构：COc1ccc(C(=O)c2ccc(C)cc2)cc1
HCID32113

Benzophenone, 4-methoxy-4'-methyl-

C15H14O2

收率 7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Clc1ccccc1
溶剂HCID7964

Chlorobenzene

C6H5Cl

PROCEDURE

实验过程

In like manner to Example 8, anisole and para-toluic acid were reacted together (4 hour reflux) in chlorobenzene in the presence of ytterbium (III) trifluoromethanesulfonate hydrate, to give crude 4-methoxy-4′-methylbenzophenone (0.15 g, 7% yield).