Hydrazine hydrate (1:1) → Arabinosehydrazon

HRID 279931

반응식

HRID 279931 반응식
[O:1]=[CH:2][C@H:3]([C@@H:5]([C@@H:7]([CH2:9]O)[OH:8])[OH:6])[OH:4].O.[NH2:12][NH2:13]>CO>[CH:9](=[N:12][NH2:13])[C@H:7]([C@@H:5]([C@@H:3]([CH2:2][OH:1])[OH:4])[OH:6])[OH:8]

참가 물질

4

반응물 2

HCID 24654Hydrazine hydrate (1:1)HCID 66308D-Arabinose

생성물 1

HCID 86740783Arabinosehydrazon

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

A solution of 4.0 g of D-arabinose in 10 ml of methanol and 10 ml of hydrazine hydrate was stirred overnight, then evaporated to dryness in vacuo. The residue was triturated with 25 ml of methanol and the solid was collected, giving 3.5 g of D-arabinose hydrazone.

후처리

  1. customevaporated to dryness in vacuo
  2. customThe residue was triturated with 25 ml of methanol
  3. customthe solid was collected

출처 및 근거

ORD 기록
ord-ebf88657c39e4ad8abc375b13788fe63
출처 데이터셋
uspto-grants-1986_05
특허 번호
US04587331

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