Hydrochloric Acid → Tris(dimethylaminomethyl)phosphine trihydrochloride
반응식
[CH3:1][N:2]([CH2:4][P:5]([CH2:10][N:11]([CH3:13])[CH3:12])[CH2:6][N:7]([CH3:9])[CH3:8])[CH3:3].[ClH:14]>C(O)C>[ClH:14].[ClH:14].[ClH:14].[CH3:3][N:2]([CH2:4][P:5]([CH2:10][N:11]([CH3:13])[CH3:12])[CH2:6][N:7]([CH3:9])[CH3:8])[CH3:1]참가 물질
4
실험 절차
A rubber-capped serum bottle containing 25 ml of ethanol was purged of air with argon, and then charged by means of a syringe with 2.31 g (11.25 mmol) of tris(dimethylaminomethyl)phosphine and 7.00 ml (42.0 mmol) of 6 N hydrochloric acid. The solution, which fumed but remained clear, was shaken for 30 min and then stripped under vacuum, leaving 3.55 g (100% yield) of tris(dimethylaminomethyl)phosphine trihydrochloride as a white, crystalline solid.
후처리
- customwas purged of air with argon
출처 및 근거
- ORD 기록
- ord-99e16ac29cc94da39b6933c63753d264
- 출처 데이터셋
- uspto-grants-1980_09
- 특허 번호
- US04225512
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