Phosphorus oxychloride → 1-Chloro-7-methoxy-4-(2-methoxyphenyl)phthalazine

HRID 29944노트

반응식

HRID 29944 반응식
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([C:7]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=3[O:20][CH3:21])=[N:8][NH:9][C:10]2=O)=[CH:5][CH:4]=1.P(Cl)(Cl)([Cl:24])=O>>[Cl:24][C:10]1[C:11]2[C:6](=[CH:5][CH:4]=[C:3]([O:2][CH3:1])[CH:12]=2)[C:7]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[O:20][CH3:21])=[N:8][N:9]=1

참가 물질

3

반응물 2

HCID 24813Phosphorus oxychlorideHCID 692130087-methoxy-4-(2-methoxyphenyl)-2H-phthalazin-1-one

생성물 1

HCID 866122131-Chloro-7-methoxy-4-(2-methoxyphenyl)phthalazine

실험 절차

This compound is obtained according to the procedure described in 1.3. by reacting 7-methoxy-4-(2-methoxyphenyl)-2H-phthalazin-1-one with phosphoryl chloride.

후처리

  1. customThis compound is obtained

출처 및 근거

ORD 기록
ord-de4600bee0bf4f4d9301fbc6d268b00f
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07423030B2

반응 노트

불러오는 중…