Phenylacetyl chloride → 3,5-Dimethoxy-2-(phenylacetyl)benzoic acid

HRID 29966

반응식

HRID 29966 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:10]=[C:11]([O:13][CH3:14])[CH:12]=1)[C:6]([O:8]C)=[O:7].[C:15]1([CH2:21][C:22](Cl)=[O:23])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH3:1][O:2][C:3]1[C:4]([C:22](=[O:23])[CH2:21][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[C:5]([CH:10]=[C:11]([O:13][CH3:14])[CH:12]=1)[C:6]([OH:8])=[O:7]

참가 물질

3

반응물 2

HCID 7679Phenylacetyl chlorideHCID 75074Methyl 3,5-Dimethoxybenzoate

생성물 1

HCID 692138893,5-Dimethoxy-2-(phenylacetyl)benzoic acid

실험 절차

This compound is synthesized by reacting methyl 3,5-dimethoxybenzoate with phenylacetyl chloride via the Friedel-Crafts reaction, followed by saponification of the ester obtained, according to the method described in 2.1. It is used in crude form in the following reaction.

후처리

  1. customThis compound is synthesized
  2. customvia the Friedel-Crafts reaction
  3. customobtained
  4. customin the following reaction

출처 및 근거

ORD 기록
ord-f474b4227e984e3b8f420708e210bfb8
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07423030B2

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