Ethyl Acetoacetate → 2-(2-Methyl-1,3-dioxan-2-yl)ethanol

HRID 31639노트

반응식

HRID 31639 반응식
[CH2:1]([C:4]1([CH2:10][CH2:11][OH:12])[O:9][CH2:8][CH2:7][CH2:6][O:5]1)CC.C(OCC)(=O)CC(C)=O>>[CH3:1][C:4]1([CH2:10][CH2:11][OH:12])[O:9][CH2:8][CH2:7][CH2:6][O:5]1

참가 물질

3

반응물 2

HCID 8868Ethyl AcetoacetateHCID 597924352-(2-Propyl-1,3-dioxan-2-yl)ethanol

생성물 1

HCID 596567682-(2-Methyl-1,3-dioxan-2-yl)ethanol수율 49%

실험 절차

The same procedure as in the steps (8a) and (8b) of Example 8, was repeated using ethyl acetoacetate to obtain the title compound (5.4 g, total yield: 49%) as a light yellow oil.

출처 및 근거

ORD 기록
ord-f1c96fd3e135466e981fd004cf3af29f
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07425634B2

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