1,3-Dichloroacetone → 4-Chloromethyl-2-(2-furyl)oxazole

HRID 322282

반응식

[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]([NH2:8])=[O:7].[Cl:9][CH2:10][C:11]([CH2:13]Cl)=O>>[Cl:9][CH2:10][C:11]1[N:8]=[C:6]([C:2]2[O:1][CH:5]=[CH:4][CH:3]=2)[O:7][CH:13]=1

참가 물질

반응물 2

HCID 107931,3-Dichloroacetone

HCID 69108Furamide

생성물 1

HCID 220097064-Chloromethyl-2-(2-furyl)oxazole수율 47%

실험 절차

In substantially the same manner as in Reference Example 47, 2-furancarboxamide was aollowed to react with 1,3-dichloroacetone to give 4-chloromethyl-2-(2-furyl)oxazole. The yield was 47%. Oily substance.

출처 및 근거

ORD 기록: ord-a3a7a58566c24585b29f4c2dc2214ffc
출처 데이터셋: uspto-grants-2001_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06211215B1

연결된 노트

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