Triethylamine → HCID 22003670, 화합물
반응식
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[C:15](=[O:16])[C:10]3[N:11]=[C:12]([CH3:14])[S:13][C:9]=3[CH2:8][CH2:7][C:6]=2[CH:17]=1.BrN1C(=O)CCC1=O.C(N(CC)CC)C>ClCCCl>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[C:15](=[O:16])[C:10]3[N:11]=[C:12]([CH3:14])[S:13][C:9]=3[CH:8]=[CH:7][C:6]=2[CH:17]=1참가 물질
5
실험 절차
A solution of the product from step (i) (6.05 g) in 1,2-dichloroethane (85 ml) with N-bromosuccinimide (4.1 g) was irradiated with a 500 Watt halogen lamp for 1 h. After cooling to room temperature, triethylamine (7 ml) was added with further stirring for 0.5 hours. The solvents were evaporated under reduced pressure and the residue triturated with acetone, filtered and then further washed with water and then dried under vacuum to leave the subtitle compound as a cream solid.
후처리
- customThe solvents were evaporated under reduced pressure
- customthe residue triturated with acetone
- filtrationfiltered
- washfurther washed with water
- customdried under vacuum
출처 및 근거
- ORD 기록
- ord-d10f2582a59744f2b48bac43a44d3950
- 출처 데이터셋
- uspto-grants-2001_04
- 특허 번호
- US06218376B1
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