Chlorosulfonyl isocyanate → HCID 178514073, 화합물

반응식

ClS([N:5]=[C:6]=[O:7])(=O)=O.[N-]=C=O.[NH2:11][C:12]1[N:17]([C:18]2[CH:23]=[CH:22][CH:21]=[C:20]([NH2:24])[CH:19]=2)[CH2:16][N:15]=[C:14]2[O:25][CH:26]=[CH:27][C:13]=12>>[NH2:11][C:12]1[N:17]([C:18]2[CH:23]=[CH:22][CH:21]=[C:20]([NH:24][C:6]([NH2:5])=[O:7])[CH:19]=2)[CH2:16][N:15]=[C:14]2[O:25][CH:26]=[CH:27][C:13]=12

참가 물질

반응물 3

HCID 70918Chlorosulfonyl isocyanate

HCID 105034Isocyanate

HCID 178507142HCID 178507142, 화합물

생성물 1

HCID 178514073HCID 178514073, 화합물

실험 절차

The compound was prepared following the procedure described in Example 232(b), using chlorosulfonyl isocyanate as the isocyanate of choice, and 4-Amino-3-(3-aminophenyl)furo[2,3-d]pyrimidine (10) as the diamine of choice. MS(ES) m/e 270 [M+H]+.

후처리

customThe compound was prepared

출처 및 근거

ORD 기록: ord-d0699c594224466da4a32d77eb82c0a8
출처 데이터셋: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07427623B2

반응 노트

불러오는 중…