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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Methyl Methacrylate → Allyl methacrylate

HRID 325441
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인쇄 미리보기

반응식

HRID 325441 반응식
[C:1]([O:6][CH2:7][CH:8]=[CH2:9])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:10]([O:15]C)(=[O:14])[C:11]([CH3:13])=[CH2:12].C(OOC([O-])=O)(OC(C)C)=O>C(Cl)Cl>[C:1]([O:6][CH2:7][CH:8]=[CH2:9])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:10]([O-:15])(=[O:14])[C:11]([CH3:13])=[CH2:12]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 3

HCID 6658Methyl MethacrylateHCID 7274Allyl methacrylateHCID 86738549Propan-2-yloxycarbonyloxy carbonate

생성물 2

HCID 7274Allyl methacrylateHCID 87595Methacrylate

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

The copolymer of allyl methacrylate and methacrylate was prepared by placing 5 grams of allyl methacrylate, 95 grams of methyl methacrylate, 300 milliliters of methylene chloride, and 1.0 gram of isopropyl peroxydicarbonate in a 28 ounce round bottle. The bottle was sealed. The bottle was then heated at 50 degrees Centigrade in a water bath for 18 hours. The bottle was then removed from the water bath, and the polymer isolated by extraction with methanol to precipitate polymer. The polymer was then dried under vacuum. Thereafter, the molecular weight was determined by inherent viscosity in methylene chloride versus poly(methyl methacrylate), and was found to be in excess of 500,000.

후처리

  1. customThe bottle was sealed
  2. temperatureThe bottle was then heated at 50 degrees Centigrade in a water bath for 18 hours
  3. customThe bottle was then removed from the water bath
  4. customthe polymer isolated by extraction with methanol
  5. customto precipitate polymer
  6. customThe polymer was then dried under vacuum

출처 및 근거

ORD 기록
ord-787595545ff84d99b1cee693e655dced
출처 데이터셋
uspto-grants-1984_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04440909

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