1-Dodecanol → p-Dioxanone 2,5-Morpholinedione
반응식
[O:1]1[CH2:6][CH2:5][O:4][CH2:3][C:2]1=[O:7].[NH:8]1[C:13](=[O:14])[CH2:12][O:11][C:10](=[O:15])[CH2:9]1.C(O)CCCCCCCCCCC.CCCCC(C([O-])=O)CC.CCCCC(C([O-])=O)CC.[Sn+2]>C1(C)C=CC=CC=1>[O:4]1[CH2:5][CH2:6][O:1][C:2](=[O:7])[CH2:3]1.[NH:8]1[C:13](=[O:14])[CH2:12][O:11][C:10](=[O:15])[CH2:9]1참가 물질
6
실험 절차
p-Dioxanone (20.1 g, 0.197 moles), 2,5-morpholinedione (0.7 g, 0.00609 moles), 1-dodecanol (0.0623 g, 0.000334 moles), and a catalytic amount of stannous octoate (0.51 ml of a 0.0264 M toluene solution, 0.0000135 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampoule according to the following temperature/time scheme:
후처리
- additionmagnetically mixed in
- temperaturea flame
- customvacuum dried
- customsealed glass ampoule
출처 및 근거
- ORD 기록
- ord-198f9e3fd616432f8bc5a7791a578698
- 출처 데이터셋
- uspto-grants-1984_04
- 특허 번호
- US04441496
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