Hydrochloric Acid → HCID 422140, 화합물
반응식
[CH2:1]([N:8]1[N:12]=[N:11][C:10]([C:13]([O-:15])=[O:14])=[N:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[K+].Cl>O>[CH2:1]([N:8]1[N:12]=[N:11][C:10]([C:13]([OH:15])=[O:14])=[N:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1참가 물질
4
실험 절차
Potassium 2-benzyl-2H-tetrazole-5-carboxylate (2.42 g) was suspended in water (10 ml) and the mixture was warmed until it dissolved. The solution was cooled in ice and strongly acidified by treatment with concentrated hydrochloric acid to give 2-benzyl-2H-tetrazole-5-carboxylic acid (1.46 g), m.p. 127°-130° C.
후처리
- temperaturethe mixture was warmed until it
- dissolutiondissolved
- temperatureThe solution was cooled in ice
출처 및 근거
- ORD 기록
- ord-768adb3240b84f02a94ae142d09fbd6e
- 출처 데이터셋
- uspto-grants-1984_04
- 특허 번호
- US04442115
반응 노트
불러오는 중…