Hydrochloric Acid → 5-(chloromethyl)pyrimidine-2,4(1h,3h)-dione

HRID 325770

반응식

HRID 325770 반응식
O[CH2:2][C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1.[ClH:11]>>[Cl:11][CH2:2][C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1

참가 물질

3

실험 절차

A solution of 1.4 g. (0.010 mole) of 5-hydroxymethyl uracil in 12.5 ml. of concentrated hydrochloric acid was prepared. A colorless precipitate (5-chloromethyl uracil) formed within two minutes and after about ten minutes the precipitate was collected by filtration, washed rapidly with ice cold water, dried and then suspended in 10 ml. of dimethylformamide.

출처 및 근거

ORD 기록
ord-6b035761cb7c49199778fff3e1e35582
출처 데이터셋
uspto-grants-1984_04
특허 번호
US04442290

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