Formamide → HCID 178478096, 화합물

HRID 325951노트

반응식

HRID 325951 반응식
[Cl:1][C:2]1[CH:13]=[CH:12][CH:11]=[C:10]([Cl:14])[C:3]=1[CH2:4][C:5]1[N:6]=[CH:7]O[CH:9]=1.C([NH2:17])=O>O>[Cl:1][C:2]1[CH:13]=[CH:12][CH:11]=[C:10]([Cl:14])[C:3]=1[CH2:4][C:5]1[N:6]=[CH:7][NH:17][CH:9]=1

참가 물질

4

반응물 2

HCID 713FormamideHCID 204633054-(2',6'-Dichlorobenzyl)oxazole

생성물 1

HCID 178478096HCID 178478096, 화합물

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
180 °C

실험 절차

A mixture of 10 g of 4-(2',6'-dichlorobenzyl)oxazole and 30 ml of formamide is stirred at 180° C. for 4 hours. The mixture is cooled and diluted with water. The reaction product is thereafter isolated in the same manner as described in Example 49(d).

후처리

  1. temperatureThe mixture is cooled
  2. customThe reaction product is thereafter isolated in the same manner

출처 및 근거

ORD 기록
ord-ecce5756c6044e02b7ffaa810eb17ea9
출처 데이터셋
uspto-grants-1984_04
특허 번호
US04443466

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