Tetrabromophthalic anhydride → HCID 507315, 화합물

HRID 326341

반응식

HRID 326341 반응식
[Br:1][C:2]1[C:3]([Br:15])=[C:4]([Br:14])[C:5]([Br:13])=[C:6]2[C:11](=[O:12])[O:10][C:8](=[O:9])[C:7]=12.[NH2:16][C:17]1[C:18]([F:30])=[CH:19][C:20]([Cl:29])=[C:21]([CH:28]=1)[C:22]([O:24][CH:25]([CH3:27])[CH3:26])=[O:23]>C1(C)C=CC=CC=1>[Br:13][C:5]1[C:4]([Br:14])=[C:3]([Br:15])[C:2]([Br:1])=[C:7]([C:8]([NH:16][C:17]2[CH:28]=[C:21]([C:22]([O:24][CH:25]([CH3:26])[CH3:27])=[O:23])[C:20]([Cl:29])=[CH:19][C:18]=2[F:30])=[O:9])[C:6]=1[C:11]([OH:10])=[O:12]

참가 물질

4

반응물 2

HCID 12443Tetrabromophthalic anhydrideHCID 13519894Propan-2-yl 5-amino-2-chloro-4-fluorobenzoate

생성물 1

HCID 507315HCID 507315, 화합물

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Tetrabromophthalic anhydride (6.67 g, 0.014 mole) and 1-methylethyl 5-amino-2-chloro-4-fluorobenzoate (3.33 g, 0.014 mole) were heated to reflux with stirring in about 150 ml of toluene, then left overnight at room temperature. Filtration of the reaction mixture gave the title compound, m.p. 160°-165° C. (decomp.).

후처리

  1. temperatureto reflux
  2. filtrationFiltration of the reaction mixture

출처 및 근거

ORD 기록
ord-8055ea95a4f246ebb0c3db129877e53e
출처 데이터셋
uspto-grants-1993_12
특허 번호
US05268389

연결된 노트

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