Sodium Hydroxide → HCID 23718315, 화합물

HRID 326786노트

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HRID 326786 반응식
[CH2:1]([CH:3]([CH2:13][CH3:14])[C:4]([NH:6][CH2:7][C:8]([O:10]CC)=[O:9])=[O:5])[CH3:2].[OH-].[Na+:16]>CO>[CH2:13]([CH:3]([CH2:1][CH3:2])[C:4]([NH:6][CH2:7][C:8]([O-:10])=[O:9])=[O:5])[CH3:14].[Na+:16]

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 2268387Ethyl 2-(2-ethylbutanoylamino)acetate

생성물 1

HCID 23718315HCID 23718315, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

To a solution of ethyl N-(2-ethylbutyryl)glycinate (33.73 g) in 100 mL of methanol was added 167.6 mL of 1N sodium hydroxide, and the solution stirred for 1.5 hr. Solvents were evaporated in vacuo, and then fresh methanol was added and evaporated to give 32.6 g of a pale yellow oil.

후처리

  1. customSolvents were evaporated in vacuo
  2. additionfresh methanol was added
  3. customevaporated

출처 및 근거

ORD 기록
ord-4e69deb7f80a40ca802f059a16d2cd57
출처 데이터셋
uspto-grants-1993_12
특허 번호
US05270331

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