Methanol → HCID 14880138, 화합물

HRID 326840노트

반응식

HRID 326840 반응식
[CH3:1][O:2][CH2:3][O:4][CH2:5][C:6]#[N:7].[Na].[CH3:9][OH:10]>>[CH3:1][O:2][CH2:3][O:4][CH2:5][C:6](=[NH:7])[O:10][CH3:9]

참가 물질

4

반응물 3

HCID 887MethanolHCID 5360545SodiumHCID 19736216(Methoxymethoxy)acetonitrile

생성물 1

HCID 14880138HCID 14880138, 화합물

실험 절차

Obtained using the procedure described in section a of Example 2, starting with 286.8 g (2.84 moles) of methoxymethoxyacetonitrile [prepared according to D. J. Loder and W. M. Bruner, U.S. Pat. No. 2,398,757; C.A. 1946, 40, 3774] and 6.5 g (0.284 gram-atom) of sodium in 1430 ml of methanol. Reaction time: 2 days. Yld: 302.6 g (80%), b.p.15 62°-65° C.

후처리

  1. customObtained
  2. customprepared
  3. customReaction time
  4. custom2 days
  5. custom302.6 g (80%), b.p.15 62°-65° C.

출처 및 근거

ORD 기록
ord-7d41e234c6214dbbbb2e4e714ad9efd2
출처 데이터셋
uspto-grants-1993_12
특허 번호
US05270465

반응 노트

불러오는 중…