Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Aminopyrazine-2-carbonitrile → 4-Amino-2-(methoxymethoxymethyl)pteridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Aminopyrazine-2-carbonitrile | HCID 817699 | — |
| 반응물 | 2-(Methoxymethoxy)acetamidine | HCID 10534653 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-Amino-2-(methoxymethoxymethyl)pteridine | HCID 10680492 | — |
반응 단계
Obtained using the procedure described in section c of Example 2, starting with 12.0 g (0.10 mole) of 3-amino-2-pyrazinecarbonitrile and 18.0 g (0.15 mole) of 2-(methoxymethoxy)acetamidine in 400 ml of absolute ethanol. Refluxing time: 4 hours. Yld: 15.8 g (71%), m.p. 129°-131° C. (ethanol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05270465 |
| 출처 데이터셋 | uspto-grants-1993_12 |
| ORD ID | ord-241ab9556c384a10bcd413f22b1519f1 |
| 출처 메모 | uspto-grants-1993_12 |