Ethanol → 2-Isopropoxymethyl-4(3H)-pteridinone
반응식
N[C:2]1[C:11]2[C:6](=[N:7][CH:8]=[CH:9][N:10]=2)[N:5]=[C:4]([CH2:12][O:13][CH:14]([CH3:16])[CH3:15])[N:3]=1.C([OH:19])C>[OH-].[Na+]>[CH:14]([O:13][CH2:12][C:4]1[NH:3][C:2](=[O:19])[C:11]2[C:6](=[N:7][CH:8]=[CH:9][N:10]=2)[N:5]=1)([CH3:16])[CH3:15]참가 물질
4
실험 절차
Obtained using the procedure described in section d of Example 2, starting with 4.5 g (0.0205 mole) of 4-amino-2-(isopropoxymethyl)pteridine in 150 ml of 5% aqueous sodium hydroxide. Heating time: 2 hours at 80° C. Yld: 3.0 g (66%), m.p. 198°-199° C. (ethanol).
후처리
- customObtained
- temperatureHeating time
- custom2 hours
- customat 80° C
출처 및 근거
- ORD 기록
- ord-15c16d4e0c0b495d98afbcfc12788beb
- 출처 데이터셋
- uspto-grants-1993_12
- 특허 번호
- US05270465
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