Chloride → Magnesium Glycinate

HRID 328559

반응식

HRID 328559 반응식
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].C(=O)([O-])[O-].[Mg+2:10].[Cl-].Cl[O-].[Al+3].Cl[O-].Cl[O-]>O>[NH2:1][CH2:2][C:3]([O-:5])=[O:4].[Mg+2:10].[NH2:1][CH2:2][C:3]([O-:5])=[O:4]

참가 물질

6

반응물 4

HCID 312ChlorideHCID 750GlycineHCID 11029Magnesium CarbonateHCID 22096649Aluminum chlorhydroxide

생성물 1

HCID 84645Magnesium Glycinate

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
75 °C

실험 절차

Magnesium glycinate was prepared by reacting 4 grams of glycine with 2.5 grams of basic magnesium carbonate (26.3% Mg) in 30 grams of water while agitating at 75° C. for one half hour. The cooled mixture was then added to 77 grams of zirconyl chloride (13.6% Zr) with stirring. To the above solution 100 grams of 50% aluminum chlorhydroxide (12.5% Al) was added with agitation. The mixture was heated at 85° C. for 20 minutes. The product was then evaporated at 53° C. under a vacuum of 200 mm of Hg and contained 15.8% Al, 13.6% Mg. 5.3% glycine and 22.1% Cl.

후처리

  1. stirringwith stirring
  2. temperatureThe mixture was heated at 85° C. for 20 minutes
  3. customThe product was then evaporated at 53° C. under a vacuum of 200 mm of Hg

출처 및 근거

ORD 기록
ord-f3633a8a53cf4448a4418701373d167d
출처 데이터셋
uspto-grants-1977_04
특허 번호
US04017599

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