Azelaic Acid → Diprop-1-en-2-yl nonanedioate

HRID 329247

반응식

HRID 329247 반응식
[C:1]([OH:13])(=[O:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10]>C(Cl)Cl>[C:1]([O:13][C:5]([CH3:6])=[CH2:4])(=[O:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([O:11][C:2]([CH3:3])=[CH2:1])=[O:10]

참가 물질

3

반응물 1

HCID 2266Azelaic Acid

생성물 1

HCID 23466330Diprop-1-en-2-yl nonanedioate

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

Azelaic acid (100 grams, 0.53 mole), methylene chloride (500 ml.) and mercuric acetate (18.2 grams, 0.057 mole) are treated with 1 ml. of boron trifluoride etherate, and propyne gas is bubbled through the mixture for 3 hours. Solid sodium bicarbonate (5 grams) is added, and the mixture is filtered free of solids and metallic mercury.

후처리

  1. customof boron trifluoride etherate, and propyne gas is bubbled through the mixture for 3 hours
  2. additionSolid sodium bicarbonate (5 grams) is added
  3. filtrationthe mixture is filtered free of solids and metallic mercury

출처 및 근거

ORD 기록
ord-7e0bf1f8d03f4384b7b8d833b3bfe3a2
출처 데이터셋
uspto-grants-1977_04
특허 번호
US04020123

연결된 노트

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