3-Phenylprop-2-Enal → HCID 346108, 화합물

HRID 330350노트

반응식

HRID 330350 반응식
[CH:1](=O)[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[C:11]([NH:19][NH2:20])(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>CO>[C:11]([NH:19][N:20]=[CH:1][CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

참가 물질

4

반응물 2

HCID 3073-Phenylprop-2-EnalHCID 11955Benzoylhydrazine

생성물 1

HCID 346108HCID 346108, 화합물수율 88%

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

To 200 ml of methanol solution containing 13.2 g of cinnamaldehyde was added 13.6 g of benzoylhydrazine, followed by stirring for 30 minutes at room temperature, for the precipitation of crystals. The crystals were filtered off and dried. Thus there was obtained 22 g of cinnamaldehyde benzoyl hydrazone (mp. 192°-194° C.).

후처리

  1. filtrationThe crystals were filtered off
  2. customdried

출처 및 근거

ORD 기록
ord-e79f7a0de29b4c88b50afa4aa0c8a206
출처 데이터셋
uspto-grants-1990_01
특허 번호
US04895947

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