Methyl iodide → HCID 178480658, 화합물

HRID 333020

반응식

HRID 333020 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[CH:11][N:10]=[CH:9]2)=[CH:4][CH:3]=1.[CH3:13][I:14]>C1COCC1>[I-:14].[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([N+:8]2[CH:12]=[CH:11][N:10]([CH3:13])[CH:9]=2)=[CH:6][CH:7]=1

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 1428591-(4-Chlorophenyl)-1H-imidazole

생성물 1

HCID 178480658HCID 178480658, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

1-(4-Chlorophenyl)imidazole (0.37 g, 2.07 mmol) is dissolved in THF (5 ml) and subsequently admixed with methyl iodide (1.47 g, 10.4 mmol) and allowed to stand for 20 hours. The precipitate formed is subsequently filtered off and washed with ethanol and with petroleum ether and subsequently dried under reduced pressure. This gives 0.46 g of 1-(4-chlorophenyl)-3-methylimidazolium iodide.

후처리

  1. customThe precipitate formed
  2. filtrationis subsequently filtered off
  3. washwashed with ethanol and with petroleum ether
  4. customsubsequently dried under reduced pressure

출처 및 근거

ORD 기록
ord-676487415dcd4a69a0c42a1697107604
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08877937B2

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