Formic Acid → HCID 178420610, 화합물
반응식
[N:1]1[C:6](C=O)=[CH:5][CH:4]=[CH:3][C:2]=1C=O.[NH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(O)=O>C(O)C>[C:12]1([N:11]=[C:6]2[CH2:5][CH:4]=[CH:3][C:2](=[N:11][C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[NH:1]2)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1참가 물질
5
실험 절차
2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).
후처리
- filtrationThe product was filtered
- washwashed with cold ethanol
- customdried in a vacuum oven (50° C.) overnight
출처 및 근거
- ORD 기록
- ord-21efaacccac443d7a83aa3e70255ab54
- 출처 데이터셋
- uspto-grants-2008_09
- 특허 번호
- US07429684B2
반응 노트
불러오는 중…