Formic Acid → HCID 178420610, 화합물

HRID 33818

반응식

HRID 33818 반응식
[N:1]1[C:6](C=O)=[CH:5][CH:4]=[CH:3][C:2]=1C=O.[NH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(O)=O>C(O)C>[C:12]1([N:11]=[C:6]2[CH2:5][CH:4]=[CH:3][C:2](=[N:11][C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[NH:1]2)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

참가 물질

5

반응물 3

HCID 284Formic AcidHCID 6115AnilineHCID 794852,6-Diformylpyridine

생성물 1

HCID 178420610HCID 178420610, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).

후처리

  1. filtrationThe product was filtered
  2. washwashed with cold ethanol
  3. customdried in a vacuum oven (50° C.) overnight

출처 및 근거

ORD 기록
ord-21efaacccac443d7a83aa3e70255ab54
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07429684B2

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